ICSSCCET 2015

International Conference on Systems, Science, Control, Communication, Engineering and Technology 2015

 


ICSSCCET 2015 Kokula Krishna Hari K
Publication Meta Value
Short Title ICSSCCET 2015
Publisher ASDF, India
ISBN 13 978-81-929866-1-6
ISBN 10 81-929866-1-6
Language English
Type Hard Bound - Printed Book
Copyrights ICSSCCET Organizers / DCRC, London, UK
Editor-in-Chief Ramachandran T
Conference Dates 10 - 11, August 2015
Venue Country Karpagam Institute of Technology, Coimbatore, India
Submitted Papers 410
Acceptance Rate 4.11%
Website www.icssccet.org

Paper 047


Characterization of Nickel Oxide Nanoparticles Synthesized via solution-phase Precursor Route

Characterization of Nickel Oxide Nanoparticles Synthesized via solution-phase Precursor Route

A Lathamaragatham1

1Department of Science and humanities (Physics),
Karpagam Institute of Technology, Coimbatore, India

Abstract

Nickel oxide (NiO) nanoparticles were produced via a solution-phase precursor route by adding solid Guanidium carbonate in citric acid and nickel nitrate hexahydrate solution at the temperature of 95 °C in water bath. High purity NiO nanoparticles were obtained by calcinating the precipitated powders at different temperatures. Thermal analysis reveals the phase formation temperature by degrading the citrates and water content before 500oC. The strong absorption band at 419 cm-1 is corresponding to the stretching vibration of NiO are confirmed by FTIR spectrum. X-ray diffraction patterns revealed that the well-crystallized/high-purity nanostructure with grain size ~35 nm of NiO nanoparticles. Scanning electron microscope and FESEM images showed that the synthesized NiO nanopowder had porous structure with pore size of ~90 nm. Nowadays porous nanopowders are using for the applications of super capacitors.

Author's Profile

A Lathamaragatham : Profile

Cite this Article as Follows

A Lathamaragatham."Characterization of Nickel Oxide Nanoparticles Synthesized via solution-phase Precursor Route." International Conference on Systems, Science, Control, Communication, Engineering and Technology (2015): 216-220. Print.